Dicyclohexyl succinate

Base Information

• Chemical Name: Dicyclohexyl succinate
• CAS No.: 965-40-2
• Molecular Formula: C16H26 O4
• Molecular Weight: 282.37524
• Hs Code.: 2917190090
• NSC Number: 406609
• DSSTox Substance ID: DTXSID30242279
• Wikidata: Q83125916
• Mol file: 965-40-2.mol

Synonyms:butanedioic acid dicyclohexyl ester;dicyclohexyl succinate;succinic acid dicyclohexyl ester

Chemical Property of Dicyclohexyl succinate

Chemical Property:

• Vapor Pressure: 6.41E-06mmHg at 25°C
• Boiling Point: 378.2°Cat760mmHg
• Flash Point: 182.2°C
• PSA: 52.60000
• Density: 1.07g/cm³
• LogP: 3.51840
• XLogP3: 3.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 7
• Exact Mass: 282.18310931
• Heavy Atom Count: 20
• Complexity: 282

Purity/Quality:

99%, ^*data from raw suppliers

SUCCINIC ACIDDICYCLOHEXYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC(CC1)OC(=O)CCC(=O)OC2CCCCC2

Technology Process of Dicyclohexyl succinate

There total 4 articles about Dicyclohexyl succinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

dicyclohexyl trans-butenedioate (621-13-6,135607-72-6,47092-64-8) → anhydrous cyclohexyl succinate (965-40-2)

Guidance literature:

With [CpCoCpNMe₂][OTf]; tert-butylammonium hexafluorophosphate(V); toluene-4-sulfonic acid; In 1,2-dimethoxyethane; for 48h; Kinetics; Electrochemical reaction;

DOI:10.1021/jacs.1c03335

Reference yield:

succinic acid (110-15-6) + cyclohexanol (108-93-0) → anhydrous cyclohexyl succinate (965-40-2)

Guidance literature:

With toluene-4-sulfonic acid; benzene; unter Entfernen des entstehenden Wassers;

Reference yield:

succinoyl dichloride (543-20-4) + cyclohexanol (108-93-0) → anhydrous cyclohexyl succinate (965-40-2)

Guidance literature:

With pyridine;

upstream raw materials:

succinoyl dichloride

cyclohexanol

succinic acid

dicyclohexyl trans-butenedioate

Downstream raw materials:

2-[(E)-2-(3-(1-carboxy cyclohexylacetylamino)phenyl)ethenyl]-6-[4-(4-bromophenyl) butoxy]methylpyridine

Refernces

• 1、 Perkel',Freidin,Neginskaya,Stolyankova,Ivanova. "NONCHAIN CONVERSION OF alpha -DIKETONES AND TRANSACYLATION OF CARBOXYLIC-ACID ANHYDRIDES UNDER AUTOXIDATION CONDITIONS.". . p. 1444 - 1449. Retrieved 2007/10/02.