Difluoromethylbis(trifluoromethyl)amine

Base Information

• Chemical Name: Difluoromethylbis(trifluoromethyl)amine
• CAS No.: 73563-15-2
• Molecular Formula: C3HF8N
• Molecular Weight: 203.034
• DSSTox Substance ID: DTXSID70223764
• Nikkaji Number: J857.003E
• Wikidata: Q83102258
• Mol file: 73563-15-2.mol

Synonyms:Difluoromethylbis(trifluoromethyl)amine;73563-15-2;(CF3)2NCHF2;DTXSID70223764;BOXXLRRPGNOFCW-UHFFFAOYSA-N

Chemical Property of Difluoromethylbis(trifluoromethyl)amine

Chemical Property:

• Vapor Pressure: 1520mmHg at 25°C
• Boiling Point: 6.1°Cat760mmHg
• Flash Point: °C
• Density: 1.569g/cm³
• XLogP3: 3.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 9
• Rotatable Bond Count: 1
• Exact Mass: 202.99812433
• Heavy Atom Count: 12
• Complexity: 129

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(N(C(F)(F)F)C(F)(F)F)(F)F

Technology Process of Difluoromethylbis(trifluoromethyl)amine

There total 2 articles about Difluoromethylbis(trifluoromethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trimethylamine (75-50-3) → perfluorotrimethylamine (432-03-1) + Heptafluorotrimethylamine (73551-02-7) + 1,1-Difluor-N,N-bis(trifluormethyl)methanamin (73563-15-2) + hexafluortrimetylamin

Guidance literature:

With hydrogen fluoride; at -10 ℃; Further byproducts given; electrofluorination;

DOI:10.1016/S0022-1139(00)82579-8

Reference yield:

tetramethlyammonium chloride (75-57-0) → perfluorotrimethylamine (432-03-1) + perfluoro(dimethylethylamine) (815-28-1) + Heptafluorotrimethylamine (73551-02-7) + 1,1-Difluor-N,N-bis(trifluormethyl)methanamin (73563-15-2)

Guidance literature:

With hydrogen fluoride; for 90h; Further byproducts given. Title compound not separated from byproducts; 5-6 V, 2.5 A dm^-2, 900 A h,;

DOI:10.1016/S0022-1139(96)03550-6

upstream raw materials:

trimethylamine

tetramethlyammonium chloride

Refernces

• 1、 Buerger, H.,Niepel, H.,Pawelke, G.,Frohn, H. J.,Sartori, P.. "HEXA-, HEPTA- UND OCTAFLUORTRIMETHYLAMIN". . p. 231 - 238. Retrieved 2007/10/02.