Technology Process of iron meso-tetrakis(heptafluorobutyramidophenyl)porphyrin bromide
There total 1 articles about iron meso-tetrakis(heptafluorobutyramidophenyl)porphyrin bromide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen bromide;
In
tetrahydrofuran; benzene;
heating with 2,6-lutidine in an oil bath at 80°C, 3h; cooling toroom temp; exposing to air; addn. of CHCl3; pouring into separatory funnel containing water; washing aq. layer with CHCl3; drying organic extracts (Na2SO4); evapn.;flash chromy. (silica gel, CHCl3, CHCl3/CH3OH 9/1); evapn.; dissoln. inchloroform; addn. of concd. HBr; stirring, 2h; washing (H2O); drying (Na2SO4); evapn.; recystn.; elem. anal.;
