Technology Process of (RS)-2-(3,7-dimethyloctyl)benzoic acid
There total 6 articles about (RS)-2-(3,7-dimethyloctyl)benzoic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3-(2,6-dimethylheptyl)phthalide;
With
di-tert-butyl peroxide; HSiPh3;
at 140 ℃;
for 5h;
With
hydrogenchloride;
In
diethyl ether;
for 70h;
DOI:10.1021/jo060481q
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: H2
2.1: sodium iodide / acetone / 1 h / Heating
3.1: magnesium / diethyl ether / 20 °C
3.2: 50 percent / diethyl ether; tetrahydrofuran / 3 h / 20 °C
4.1: triphenylsilane; di-tert-butyl peroxide / 5 h / 140 °C
4.2: 36 percent / hydrochloric acid / diethyl ether / 70 h
With
di-tert-butyl peroxide; hydrogen; magnesium; sodium iodide; HSiPh3;
In
diethyl ether; acetone;
2.1: Hunsdiecker reaction;
DOI:10.1021/jo060481q
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium iodide / acetone / 1 h / Heating
2.1: magnesium / diethyl ether / 20 °C
2.2: 50 percent / diethyl ether; tetrahydrofuran / 3 h / 20 °C
3.1: triphenylsilane; di-tert-butyl peroxide / 5 h / 140 °C
3.2: 36 percent / hydrochloric acid / diethyl ether / 70 h
With
di-tert-butyl peroxide; magnesium; sodium iodide; HSiPh3;
In
diethyl ether; acetone;
DOI:10.1021/jo060481q