1-bromo-2,3-epoxy-4-phenylbutane

Base Information Edit

Chemical Name:1-bromo-2,3-epoxy-4-phenylbutane
CAS No.:511553-23-4
Molecular Formula:C₁₀H₁₁BrO
Molecular Weight:227.101
Hs Code.:
Mol file:511553-23-4.mol

Synonyms:1-bromo-2,3-epoxy-4-phenylbutane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-bromo-2,3-epoxy-4-phenylbutane Edit

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Technology Process of 1-bromo-2,3-epoxy-4-phenylbutane

There total 2 articles about 1-bromo-2,3-epoxy-4-phenylbutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 40734-75-6
(E)-(4-bromobut-2-en-1-yl)benzene

: 511553-23-4
1-bromo-2,3-epoxy-4-phenylbutane

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃;
DOI:10.1021/ja020761x

Reference yield:

: 42238-15-3,22910-59-4,49676-93-9
(2E)-4-phenylbut-2-en-1-ol

: 511553-23-4
1-bromo-2,3-epoxy-4-phenylbutane

Guidance literature:: Multi-step reaction with 2 steps

1: N-bromosuccinimide; dimethylsulphide / CH₂Cl₂ / 3 h / -30 - 20 °C

2: 52 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 20 °C

With N-Bromosuccinimide; dimethylsulfide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/ja020761x