Technology Process of 3-(3,4-dihydroxyphenyl)propyl acetate
There total 7 articles about 3-(3,4-dihydroxyphenyl)propyl acetate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3-(4'-hydroxyphenyl)-1-propyl acetate;
With
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
methanol;
at 0 ℃;
for 1h;
With
sodium dithionite;
In
water;
at 20 ℃;
for 0.0833333h;
DOI:10.1021/jf301131a
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine; dmap / dichloromethane / 20 °C
2: tetrahydrofuran / 0 - 20 °C / Inert atmosphere
3: triethylamine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere
5: 5%-palladium/activated carbon; hydrogen / methanol / 20 °C / Inert atmosphere
With
dmap; 5%-palladium/activated carbon; tetrabutyl ammonium fluoride; hydrogen; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.ejmech.2014.01.016
