Technology Process of 2β-hydroxy-3α-phenylthio-<3β-(2)H>-5α-cholestane
There total 4 articles about 2β-hydroxy-3α-phenylthio-<3β-(2)H>-5α-cholestane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
dichloromethane;
for 0.25h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 84 percent / methan(2)H-ol, sodium borodeuteride / 1 h / Ambient temperature
2: 56 percent / zinc powder, acetic acid / 0.5 h
3: 62 percent / lead tetra-acetate / CH2Cl2 / 0.5 h / -40 °C
4: 81 percent / methanolic sodium hydroxide / CH2Cl2 / 0.25 h / Ambient temperature
With
lead(IV) acetate; sodium hydroxide; sodium borodeuteride; deuteromethanol; acetic acid; zinc;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 62 percent / lead tetra-acetate / CH2Cl2 / 0.5 h / -40 °C
2: 81 percent / methanolic sodium hydroxide / CH2Cl2 / 0.25 h / Ambient temperature
With
lead(IV) acetate; sodium hydroxide;
In
dichloromethane;
