3^A-amino-3^A-deoxy-β-cyclodextrin

Base Information

• Chemical Name: 3^A-amino-3^A-deoxy-β-cyclodextrin
• CAS No.: 125827-01-2
• Molecular Formula: C₄₂H₇₁NO₃₄
• Molecular Weight: 1134.01
• Mol file: 125827-01-2.mol

Synonyms:3^A-amino-3^A-deoxy-β-cyclodextrin

Chemical Property of 3^A-amino-3^A-deoxy-β-cyclodextrin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3^A-amino-3^A-deoxy-β-cyclodextrin

There total 3 articles about 3^A-amino-3^A-deoxy-β-cyclodextrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

3A-azido-3A-deoxy-altro-β-cyclodextrin (161523-00-8) → (2AS,3AS)-3A-amino-3A-deoxy-3A-β-cyclodextrin (125827-01-2,117194-77-1)

Guidance literature:

3^A-azido-3^A-deoxy-altro-β-cyclodextrin; With triphenylphosphine; In N,N-dimethyl-formamide; at 40 ℃; for 24h;

With ammonium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

DOI:10.1021/jo035229m

Reference yield:

C62H97NO34 → all-trans-Retinal (116-31-4) + 3A-amino-3A-deoxy-β-cyclodextrin (125827-01-2)

Guidance literature:

With water; In various solvent(s); at 25 ℃; pH=4.0; Further Variations:; Reagents; Kinetics;

DOI:10.1016/j.bmcl.2005.12.052

Reference yield:

β-cyclodextrin-2,3-mannoepoxide (84648-78-2) → (2AS,3AS)-3A-amino-3A-deoxy-3A-β-cyclodextrin (125827-01-2,117194-77-1)

Guidance literature:

With ammonium hydroxide; at 60 ℃; for 3h; Yield given;

DOI:10.1246/cl.1988.553

upstream raw materials:

β-cyclodextrin-2,3-mannoepoxide

3^A-azido-3^A-deoxy-altro-β-cyclodextrin

Downstream raw materials:

C₅₁H₇₇NO₃₇

Refernces

• 1、 Yuan, De-Qi,Tahara, Tsutomu,Chen, Wen-Hua,Okabe, Yuji,Yang, Cheng,Yagi, Youichi,Nogami, Yasuyoshi,Fukudome, Makoto,Fujita, Kahee. "Functionalization of Cyclodextrins via Reactions of 2,3-Anhydrocyclodextrins". . p. 9456 - 9466. Retrieved 2007/10/03.