o-(trimethylgermyl)(2,3-dimethyl-3-butenyl)dimethylsilylbenzene

Base Information

• Chemical Name: o-(trimethylgermyl)(2,3-dimethyl-3-butenyl)dimethylsilylbenzene
• CAS No.: 136266-29-0
• Molecular Formula: C₁₇H₃₀GeSi
• Molecular Weight: 335.101
• Mol file: 136266-29-0.mol

Synonyms:o-(trimethylgermyl)(2,3-dimethyl-3-butenyl)dimethylsilylbenzene

Chemical Property of o-(trimethylgermyl)(2,3-dimethyl-3-butenyl)dimethylsilylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of o-(trimethylgermyl)(2,3-dimethyl-3-butenyl)dimethylsilylbenzene

There total 1 articles about o-(trimethylgermyl)(2,3-dimethyl-3-butenyl)dimethylsilylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

dimethylphenyl(trimethylgermyl)silane (37865-47-7) + 2,3-dimethyl-buta-1,3-diene (513-81-5) → o-(trimethylgermyl)(2,3-dimethyl-3-butenyl)dimethylsilylbenzene (136266-29-0) + Dimethylphenylsilane (766-77-8) + 1,1,3,3-tetramethyl-1,3-diphenyldisiloxane (56-33-7) + trimethylgermane (1449-63-4) + (2,3-dimethyl-3-butenyl)dimethylphenylsilane (98213-22-0)

Guidance literature:

In cyclohexane; Irradiation (UV/VIS); irradiation of catenate in cyclohexane containing a large excess of 2,3-dimethylbutadiene as trapping agent with a 110 W low pressure Hg arc lamp at room temp. under Ar for 1-4 h; identification by GC and GC-MS;

DOI:10.1016/0022-328X(91)86036-P

upstream raw materials:

dimethylphenyl(trimethylgermyl)silane

2,3-dimethyl-buta-1,3-diene

Refernces