Technology Process of C21H25NO
There total 9 articles about C21H25NO which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C14H17NO; benzyl bromide;
In
acetonitrile;
at 20 ℃;
for 2h;
With
methanol; sodium tetrahydroborate;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione / tetrahydrofuran / 0.5 h / 20 °C
2.1: potassium hydroxide / tetrahydrofuran / 1 h / 20 °C
3.1: indium(III) chloride / tetrahydrofuran / 0.75 h / 25 °C / Inert atmosphere
4.1: methanol / 1.5 h / 30 °C / Inert atmosphere
5.1: acetonitrile / 2 h / 20 °C
5.2: 20 °C
With
1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; potassium hydroxide;
indium(III) chloride;
In
tetrahydrofuran; methanol; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium tetrahydroborate; methanol / 2 h / Reflux
2.1: toluene-4-sulfonic acid / tetrahydrofuran / 1 h / Reflux
3.1: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione / tetrahydrofuran / 0.5 h / 20 °C
4.1: potassium hydroxide / tetrahydrofuran / 1 h / 20 °C
5.1: indium(III) chloride / tetrahydrofuran / 0.75 h / 25 °C / Inert atmosphere
6.1: methanol / 1.5 h / 30 °C / Inert atmosphere
7.1: acetonitrile / 2 h / 20 °C
7.2: 20 °C
With
methanol; sodium tetrahydroborate; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; toluene-4-sulfonic acid; potassium hydroxide;
indium(III) chloride;
In
tetrahydrofuran; methanol; acetonitrile;
