Technology Process of 2,5-Furandione,3-ethyl-4-methyl-
There total 12 articles about 2,5-Furandione,3-ethyl-4-methyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide; water;
In
ethanol;
at 20 ℃;
for 0.5h;
- Guidance literature:
-
C10H15Cl2NOS;
With
N,N,N,N,-tetramethylethylenediamine; sodium carbonate; copper(l) chloride;
In
acetonitrile;
at 30 ℃;
for 16h;
Inert atmosphere;
With
water;
In
acetonitrile;
Further stages;
Inert atmosphere;
DOI:10.1016/j.tet.2012.04.117
- Guidance literature:
-
2,3-Dimethylmaleic anhydride;
With
N-Bromosuccinimide;
In
tetrachloromethane;
at 88 ℃;
for 3.5h;
methylmagnesium bromide;
With
N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide;
In
tetrahydrofuran;
at -5 - 5 ℃;
Temperature;
Concentration;
Inert atmosphere;