(S)-(-)-1-Acetoxy-4-isopropyl-1-cyclohexene

Base Information Edit

Chemical Name:(S)-(-)-1-Acetoxy-4-isopropyl-1-cyclohexene
CAS No.:132042-14-9
Molecular Formula:C₁₁H₁₈O₂
Molecular Weight:182.263
Hs Code.:
Mol file:132042-14-9.mol

Synonyms:(S)-(-)-1-Acetoxy-4-isopropyl-1-cyclohexene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-(-)-1-Acetoxy-4-isopropyl-1-cyclohexene Edit

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Technology Process of (S)-(-)-1-Acetoxy-4-isopropyl-1-cyclohexene

There total 3 articles about (S)-(-)-1-Acetoxy-4-isopropyl-1-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 132077-84-0
(S)-(-)-1-Acetoxy-4-isopropenyl-1-cyclohexene

: 132042-14-9
(S)-(-)-1-Acetoxy-4-isopropyl-1-cyclohexene

Guidance literature:: With Wilkinson's catalyst; hydrogen; In benzene;
DOI:10.1039/c39900001706

Reference yield:

: 38651-65-9
(1R,5S)-(+)-nopinone

: 132042-14-9
(S)-(-)-1-Acetoxy-4-isopropyl-1-cyclohexene

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / AcOH, BF₃*Et₂O / 40 h / Ambient temperature

2: 97 percent / toluene / 500 °C

3: 93 percent / H₂ / (Ph₃P)3RhCl / benzene / 15 h / 760 Torr

With boron trifluoride diethyl etherate; hydrogen; acetic acid; Wilkinson's catalyst; In toluene; benzene;
DOI:10.1055/s-1992-26297

Reference yield:

: 132042-13-8
(S)-(-)-1-Acetoxy-4-(1-acetoxy-1-methylethyl)-1-cyclohexene

: 132042-14-9
(S)-(-)-1-Acetoxy-4-isopropyl-1-cyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / toluene / 500 °C

2: 93 percent / H₂ / (Ph₃P)3RhCl / benzene / 15 h / 760 Torr

With hydrogen; Wilkinson's catalyst; In toluene; benzene;
DOI:10.1055/s-1992-26297