2-Dodecen-1-ylsuccinic anhydride

Base Information

• Chemical Name: 2-Dodecen-1-ylsuccinic anhydride
• CAS No.: 19780-11-1
• Deprecated CAS: 1338799-03-3
• Molecular Formula: C16H26O3
• Molecular Weight: 266.381
• Hs Code.: 2917190090
• European Community (EC) Number: 243-296-9
• UNII: S63TTA7G5P
• Nikkaji Number: J120.744J,J149.584D
• Wikidata: Q27288708
• ChEMBL ID: CHEMBL87310
• Mol file: 19780-11-1.mol

Synonyms:19780-11-1;2-Dodecen-1-ylsuccinic anhydride;(2-Dodecenyl)succinic anhydride;2-Dodecen-1-yl succinic anhydride;CCRIS 4810;2,5-Furandione, 3-(2-dodecenyl)dihydro-;3-(2-Dodecenyl)succinic anhydride;EINECS 243-296-9;UNII-U3Z29QTW3P;S63TTA7G5P;CHEMBL87310;Succinic anhydride, (2-dodecenyl)- (8CI);2,5-Furandione, 3-dodecenyl-;3-(Dodec-2-en-1-yl)dihydrofuran-2,5-dione;2,5-Furandione, 3-(2-dodecen-1-yl)dihydro-;(2-Dodecen-1-yl)succinic anhydride;((E)-2-Dodecenyl)succinic anhydride;MFCD00005528;2-Dodecen-1-yl(-)succinic anhydride;trans-(2-Dodecenyl)succinic anhydride;428493-97-4;J149.584D;2,5-Furandione, 3-(2E)-2-dodecenyldihydro-;EC 243-296-9;2-Dodecenylsuccinic anhydride;(E)-3-(Dodec-2-en-1-yl)dihydrofuran-2,5-dione;3-(2-Dodecen-1-yl)dihydro-2,5-furandione, (2E)-;DTXCID10196504;[(E)-2-Dodecenyl]succinic anhydride;n-Dodecenyl succinic anhydride (n-DDSA);CAS-19780-11-1;DTXSID7025217;3-[(E)-dodec-2-enyl]oxolane-2,5-dione;UNII-S63TTA7G5P;U3Z29QTW3P;N-Dodecenyl succinic anhydride;UYCICMIUKYEYEU-ZHACJKMWSA-N;2-dodecen-1-yl-succinic anhydride;2-(2-Dodecenyl)succinic anhydride;AMY11737;BBA54438;Tox21_202473;Tox21_303400;BDBM50108510;LS-978;AKOS015903207;Epoxy embedding medium, hardener DDSA;CS-W010116;HY-W009400;NCGC00091241-01;NCGC00091241-02;NCGC00257398-01;NCGC00260022-01;AS-75571;PD196686;?2-DODECEN-1-YLSUCCINIC ANHYDRIDE;D0976;((E)-3-Dodec-2-enyl)-dihydro-furan-2,5-dione;(2E)-3-(2-dodecen-1-yl)dihydro-2,5-furandione;3-[(2E)-2-Dodecenyl]dihydro-2,5-furandione #;Dodecen-1-yl)succinic anhydride, (2-;(DDSA);W-107677;W-110665;Q27288708

Chemical Property of 2-Dodecen-1-ylsuccinic anhydride

Chemical Property:

• Appearance/Colour: colourless to light yellow viscous liquid
• Vapor Pressure: <1 mm Hg ( 20 °C)
• Melting Point: 41-43 °C(lit.)
• Refractive Index: 1.477
• Boiling Point: 348.398 °C at 760 mmHg
• Flash Point: 177.778 °C
• PSA: 43.37000
• Density: 0.99 g/cm³
• LogP: 4.16310
• Solubility.: 5g/L in organic solvents at 20 ℃
• Water Solubility.: 130μg/L at 25℃
• XLogP3: 5.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 10
• Exact Mass: 266.18819469
• Heavy Atom Count: 19
• Complexity: 307

Purity/Quality:

99.9% ^*data from raw suppliers

2-Dodecen-1-ylsuccinic Anhydride (cis- and trans- mixture) >95.0%(T) ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-37/39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CCCCCCCCCC=CCC1CC(=O)OC1=O
• Isomeric SMILES: CCCCCCCCC/C=C/CC1CC(=O)OC1=O
• Uses: (2-Dodecen-1-yl)succinic anhydride may be used in the following:Synthesis of amphiphilic N-[(2′-(dodec-2′-en-10-yl)succinoyl]chitosan.Chemical modification of sago starch, via esterification.Preparation of dodecenyl succinic anhydride (DDSA) gum arabic derivatives, via chemical modification of gum arabic.

Technology Process of 2-Dodecen-1-ylsuccinic anhydride

There total 1 articles about 2-Dodecen-1-ylsuccinic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 2-dodecen-1yl (?) succinic anhydride (19780-11-1)

Guidance literature:

Dodecen-(1), Maleinsaeureanhydrid;

Reference yield:

2-dodecen-1yl (?) succinic anhydride (19780-11-1) + scopolamine (51-34-3,138-12-5,64069-63-2,124917-17-5) → C33H47NO7

Guidance literature:

scopolamine; With dmap; triethylamine; In dichloromethane; for 0.666667h; Inert atmosphere;

2-dodecen-1yl (?) succinic anhydride; In dichloromethane; at 40 ℃; for 8h; Inert atmosphere;

Reference yield:

2-dodecen-1yl (?) succinic anhydride (19780-11-1) + scopolamine (51-34-3,138-12-5,64069-63-2,124917-17-5) → C63H97NO9

Guidance literature:

Multi-step reaction with 2 steps

1.1: triethylamine; dmap / dichloromethane / 0.67 h / Inert atmosphere

1.2: 8 h / 40 °C / Inert atmosphere

2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.67 h / Inert atmosphere

2.2: 12 h / 20 °C / Inert atmosphere

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane;