Technology Process of C60H77N5O16
There total 7 articles about C60H77N5O16 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C49H66N2O17;
With
oxalyl dichloride; N,N-dimethyl-formamide;
In
toluene;
at 20 ℃;
for 1.5h;
3-quinoxalin-6-yl-propylamine;
In
tetrahydrofuran; toluene;
for 0.25h;
DOI:10.1016/j.bmc.2006.01.036
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: NaH / dimethylformamide / 0.5 h / cooling
2.1: pyridine / tetrahydrofuran / 20 °C
3.1: PPh3; pyrrolidine; H2O / Pd(PPh3)4 / acetonitrile; ethyl acetate / 1 h / 20 °C
4.1: oxalyl chloride; DMF / toluene / 1.5 h / 20 °C
4.2: 94 percent / toluene; tetrahydrofuran / 0.25 h
With
pyrrolidine; pyridine; oxalyl dichloride; water; sodium hydride; N,N-dimethyl-formamide; triphenylphosphine;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/j.bmc.2006.01.036
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: H2 / Pd/C / ethanol; ethyl acetate / 1 h / 20 °C
2.1: iodotrimethylsilane / CH2Cl2 / 1 h / cooling
3.1: oxalyl chloride; DMF / toluene / 1.5 h / 20 °C
3.2: 94 percent / toluene; tetrahydrofuran / 0.25 h
With
oxalyl dichloride; trimethylsilyl iodide; hydrogen; N,N-dimethyl-formamide;
palladium on activated charcoal;
In
ethanol; dichloromethane; ethyl acetate; toluene;
DOI:10.1016/j.bmc.2006.01.036
