Technology Process of C16H14N2O2
There total 6 articles about C16H14N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-oxo-4H-chromen-3-yl trifluoromethane sulfonate; tris(4-methoxyphenyl)bismuth;
With
potassium phosphate; tetrakis(triphenylphosphine) palladium(0);
In
N,N-dimethyl-formamide;
at 90 ℃;
for 4h;
Schlenk technique;
Inert atmosphere;
With
hydrazine hydrate;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 0.5h;
Schlenk technique;
Inert atmosphere;
DOI:10.1007/s12039-018-1565-6
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine / dichloromethane / 0.17 h / 0 °C
1.2: 10 h / 20 °C
2.1: tetrakis(triphenylphosphine) palladium(0); potassium phosphate / N,N-dimethyl-formamide / 4 h / 90 °C / Schlenk technique; Inert atmosphere
2.2: 0.5 h / 20 °C / Schlenk technique; Inert atmosphere
With
potassium phosphate; tetrakis(triphenylphosphine) palladium(0); triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1007/s12039-018-1565-6
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydroxide; dihydrogen peroxide / dichloromethane / 0 - 15 °C
1.2: 1 h / 70 °C
2.1: triethylamine / dichloromethane / 0.17 h / 0 °C
2.2: 10 h / 20 °C
3.1: tetrakis(triphenylphosphine) palladium(0); potassium phosphate / N,N-dimethyl-formamide / 4 h / 90 °C / Schlenk technique; Inert atmosphere
3.2: 0.5 h / 20 °C / Schlenk technique; Inert atmosphere
With
potassium phosphate; tetrakis(triphenylphosphine) palladium(0); dihydrogen peroxide; triethylamine; sodium hydroxide;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1007/s12039-018-1565-6