undec-4t-en-6-one

Base Information

• Chemical Name: undec-4t-en-6-one
• CAS No.: 73587-64-1
• Molecular Formula: C₁₁H₂₀O
• Molecular Weight: 168.279
• Mol file: 73587-64-1.mol

Synonyms:undec-4t-en-6-one

Chemical Property of undec-4t-en-6-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of undec-4t-en-6-one

There total 3 articles about undec-4t-en-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dipentyl ketone (927-49-1) → undec-4t-en-6-one (73587-64-1,32064-74-7)

Guidance literature:

With 1-ethyl-piperidine; dichloro bis(acetonitrile) palladium(II); potassium fluoride; tin(II) trifluoromethanesulfonate; dibenzo-18-crown-6; Yield given. Multistep reaction; 1.) methylene chloride, 0 deg C, 15 min; 2.) methylene chloride, RT;

DOI:10.1246/cl.1983.1207

Reference yield:

2-methylhexanal (925-54-2) + butyraldehyde (123-72-8) → undec-4t-en-6-one (73587-64-1,32064-74-7)

Guidance literature:

With sodium hydroxide; Destillieren des Reaktionsprodukts in Gegenwart von Saeure;

Reference yield:

1-Pentyne (627-19-0) + 1-chloro-1-hexyne (1119-66-0) → undec-4t-en-6-one (73587-64-1,32064-74-7)

Guidance literature:

Multistep reaction; (i) (1,1,2-trimethyl-propyl)-borane, (ii) /BRN= 1697133/, (iii) NaOMe, (iv) H₂O₂, NaOAc;

DOI:10.1039/c39730000606

upstream raw materials:

2-methylhexanal

butyraldehyde

1-Pentyne

1-chloro-1-hexyne

Downstream raw materials:

6-undecanol

dipentyl ketone

Acetic acid 3-chloro-1-pentyl-2-phenylselanyl-hexyl ester

Refernces