Technology Process of C34H40N6O4
There total 5 articles about C34H40N6O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
acetonitrile;
at 20 ℃;
Inert atmosphere;
Cooling with ice;
DOI:10.1016/j.bmcl.2014.04.014
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogenchloride / ethanol; water / 27 h / Inert atmosphere; Reflux
2: Chiralcel AD-H column / methanol / Resolution of racemate
3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / Inert atmosphere
4: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C / Inert atmosphere; Cooling with ice
With
hydrogenchloride; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
methanol; ethanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.bmcl.2014.04.014
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 2.5 h / Inert atmosphere
2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / Inert atmosphere
3: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C / Inert atmosphere; Cooling with ice
With
dmap; sodium tris(acetoxy)borohydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1016/j.bmcl.2014.04.014
