pentafluorobenzyl 2,6-dimethylphenyl ether

Base Information

• Chemical Name: pentafluorobenzyl 2,6-dimethylphenyl ether
• CAS No.: 151503-30-9
• Molecular Formula: C₁₅H₁₁F₅O
• Molecular Weight: 302.244
• Mol file: 151503-30-9.mol

Synonyms:pentafluorobenzyl 2,6-dimethylphenyl ether

Chemical Property of pentafluorobenzyl 2,6-dimethylphenyl ether

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of pentafluorobenzyl 2,6-dimethylphenyl ether

There total 1 articles about pentafluorobenzyl 2,6-dimethylphenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2.6-dimethylphenol (576-26-1,25134-01-4) + (bromomethyl)pentafluorobenzene (1765-40-8) → pentafluorobenzyl 2,6-dimethylphenyl ether (151503-30-9)

Guidance literature:

With potassium carbonate;

DOI:10.1016/S0040-4039(00)79239-2

Reference yield: 41.0%

acetyl chloride (75-36-5) + pentafluorobenzyl 2,6-dimethylphenyl ether (151503-30-9) → Acetic acid 2,6-dimethyl-4-pentafluorophenylmethyl-phenyl ester + 3',5'-dimethyl-4'-pentafluorobenzyloxyacetophenone + Acetic acid 2,6-dimethyl-3-pentafluorophenylmethyl-phenyl ester + 2,3,4,5,6-pentafluorobenzyl chloride (653-35-0)

Guidance literature:

With aluminium trichloride; In dichloromethane; Further byproducts given; Ambient temperature;

DOI:10.1016/S0040-4039(00)79239-2

Reference yield: 41.0%

acetyl chloride (75-36-5) + pentafluorobenzyl 2,6-dimethylphenyl ether (151503-30-9) → 2,6-dimethylphenyl acetate (876-98-2) + Acetic acid 2,6-dimethyl-4-pentafluorophenylmethyl-phenyl ester + 3',5'-dimethyl-4'-pentafluorobenzyloxyacetophenone + Acetic acid 2,6-dimethyl-3-pentafluorophenylmethyl-phenyl ester + 2,3,4,5,6-pentafluorobenzyl chloride (653-35-0)

Guidance literature:

With aluminium trichloride; In dichloromethane; Mechanism; Ambient temperature; or 2,6-difluorophenol;

DOI:10.1016/S0040-4039(00)79239-2

upstream raw materials:

2.6-dimethylphenol

(bromomethyl)pentafluorobenzene

Downstream raw materials:

2,6-dimethylphenyl acetate

2,3,4,5,6-pentafluorobenzyl chloride

Refernces