Cp(molybdenum)dinitrosyl(methyl)

Base Information

• Chemical Name: Cp(molybdenum)dinitrosyl(methyl)
• CAS No.: 57034-48-7
• Molecular Formula: C₆H₈MoN₂O₂
• Molecular Weight: 236.082
• Mol file: 57034-48-7.mol

Synonyms:Cp(molybdenum)dinitrosyl(methyl)

Chemical Property of Cp(molybdenum)dinitrosyl(methyl)

Chemical Property:

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Technology Process of Cp(molybdenum)dinitrosyl(methyl)

There total 1 articles about Cp(molybdenum)dinitrosyl(methyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

ferrocenium(III) tetrafluoroborate (1282-37-7) + {Cp(molybdenum)dinitrosyl(methyl)}{cobalticinium} (111469-38-6) → ferrocene (102-54-5,55404-68-7) + Cp(molybdenum)dinitrosyl(methyl) (57034-48-7) + cobaltocenium tetrafluoroborate

Guidance literature:

In dichloromethane; Under anaerobic and anhyd. conditions, stirring of Mo-Co- and Fe-complexes in CH2Cl2 (5 min, -78°C), warming to room temp gives green soln.; Concg. in vac., gives a yellow ppt., addn. of Et2O gives further ppt. (Cp2Co)BF4. Evapn. of filtrate to dryness, column chromy. of residue (Al2O3 neutral, Et2O) gives Cp2Fe and then a green band, evapn. in vac., sublimation yields CpMo(NO)2Me.;

upstream raw materials:

ferrocenium(III) tetrafluoroborate

{Cp(molybdenum)dinitrosyl(methyl)}{cobalticinium}

Refernces