C₁₆H₁₃N

Base Information

• Chemical Name: C₁₆H₁₃N
• CAS No.: 106017-41-8
• Molecular Formula: C₁₆H₁₃N
• Molecular Weight: 219.286
• Mol file: 106017-41-8.mol

Synonyms:C₁₆H₁₃N

Chemical Property of C₁₆H₁₃N

Chemical Property:

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Technology Process of C₁₆H₁₃N

There total 1 articles about C₁₆H₁₃N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.0%

(acenaphthylene)chromium tricarbonyl (99414-44-5) + lithium isobutyronitrile (55440-70-5) → C16H13N (106017-41-8) + acenaphthylene (208-96-8,25036-01-5)

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; iodine; trifluoroacetic acid; In tetrahydrofuran; to a soln. of nucleophile in THF at -60°C soln. of complex was added, after 45 min at -60°C CF3COOH was added followed by I2, and soln. was allowed to stir overnight while being warmed to room temp.;; soln. was filtered through Celite, evapd.; residue was extd. was ether and washed with other solvents; then chromd. on silica column, eluent CH2Cl2-hexane;;

DOI:10.1021/om00145a004

upstream raw materials:

(acenaphthylene)chromium tricarbonyl

lithium isobutyronitrile

Refernces