O,N-Diethyl-N-nitrosohydroxylamine

Base Information

• Chemical Name: O,N-Diethyl-N-nitrosohydroxylamine
• CAS No.: 56235-95-1
• Molecular Formula: C4H10 N2 O2
• Molecular Weight: 118.136
• DSSTox Substance ID: DTXSID20971667
• Nikkaji Number: J61.434C
• Wikidata: Q82955240
• ChEMBL ID: CHEMBL164990
• Mol file: 56235-95-1.mol

Synonyms:O,N-Diethyl-N-nitrosohydroxylamine;BRN 1751416;N-ethoxy-N-ethylnitrous amide;N-Nitroso-O,N-diethylhydroxylamine;Hydroxylamine, O,N-diethyl-N-nitroso-;N-Nitroso-O,N-diaethylhydroxylamin [German];CHEMBL164990;DTXSID20971667;N-Nitroso-O,N-diathylhydroxylamin;N-Nitroso-O,N-diaethylhydroxylamin;AKOS006275939;3-04-00-01717 (Beilstein Handbook Reference)

Chemical Property of O,N-Diethyl-N-nitrosohydroxylamine

Chemical Property:

• Vapor Pressure: 30mmHg at 25°C
• Refractive Index: 1.4386 (estimate)
• Boiling Point: 105.1°C at 760 mmHg
• Flash Point: 17.3°C
• PSA: 67.08000
• Density: 1.03g/cm³
• LogP: 4.83050
• XLogP3: 1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 118.074227566
• Heavy Atom Count: 8
• Complexity: 67.1

Purity/Quality:

99% ^*data from raw suppliers

N-NITROSO-O,N-DIETHYL-HYDROXYLAMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(N=O)OCC

Technology Process of O,N-Diethyl-N-nitrosohydroxylamine

There total 3 articles about O,N-Diethyl-N-nitrosohydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ N-nitroso-O,N-diethyl hydroxylamine (56235-95-1)

Guidance literature:

With water; sodium nitrite;

DOI:10.1021/ja01360a049

Reference yield:

N,O-diethylhydroxylamine (4747-28-8) → N-nitroso-O,N-diethyl hydroxylamine (56235-95-1)

Guidance literature:

With nitrosating agent;

Reference yield:

N,O-diethylhydroxylamine (4747-28-8) + water (7732-18-5) → N-nitroso-O,N-diethyl hydroxylamine (56235-95-1)

Guidance literature:

DOI:10.1021/ja01360a049

upstream raw materials:

N,O-diethylhydroxylamine

water

Downstream raw materials:

ethanol

ammonium acetate

acetaldehyde

Refernces

• 1、 Meesters, A. C. M.,Rueerger, H.,Rajeswari, K.,Benn, M. H.. "THE FORMATION OF AZOXYALKANES IN REACTIONS OF SOME ORGANOMETALLIC REAGENTS WITH N-nitroso-O,N-DIALKYLHYDROXYLAMINES: THE NONPHOTOCHEMICAL SYNTHESIS OF AN ACYCLIC (E)-AZOXYALKANE". . p. 264 - 268. Retrieved 2007/10/02.