Technology Process of Naphtho[2,1,8-def]quinolin-2(1H)-one
There total 6 articles about Naphtho[2,1,8-def]quinolin-2(1H)-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
palladium on activated charcoal;
at 230 - 320 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 95 percent / NH2OH*HCl, aq. 50percent KOH / methanol / 4 h / Heating
2: 83 percent / (C2H5)3N / CH2Cl2 / 0.5 h / -20 °C
3: 51 percent / AlCl3 / CH2Cl2 / 6 h / Heating
4: 61 percent / 10percent Pd on carbon / 1 h / 230 - 320 °C
With
potassium hydroxide; aluminium trichloride; hydroxylamine hydrochloride; triethylamine;
palladium on activated charcoal;
In
methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 80 percent / HF / 24 h
2: 95 percent / NH2OH*HCl, aq. 50percent KOH / methanol / 4 h / Heating
3: 83 percent / (C2H5)3N / CH2Cl2 / 0.5 h / -20 °C
4: 51 percent / AlCl3 / CH2Cl2 / 6 h / Heating
5: 61 percent / 10percent Pd on carbon / 1 h / 230 - 320 °C
With
potassium hydroxide; aluminium trichloride; hydrogen fluoride; hydroxylamine hydrochloride; triethylamine;
palladium on activated charcoal;
In
methanol; dichloromethane;