Dibenz[a,j]acridine

Base Information

• Chemical Name: Dibenz[a,j]acridine
• CAS No.: 224-42-0
• Molecular Formula: C21H13 N
• Molecular Weight: 279.341
• Hs Code.: 2933990090
• European Community (EC) Number: 635-000-5
• NSC Number: 114903
• UNII: 088X9K64S8
• DSSTox Substance ID: DTXSID4059758
• Nikkaji Number: J2.975K
• Wikidata: Q26840806
• NCI Thesaurus Code: C44368
• Mol file: 224-42-0.mol

Synonyms:dibenz(a,h)acridine;dibenz(a,j)acridine;dibenzacridine

Chemical Property of Dibenz[a,j]acridine

Chemical Property:

• Vapor Pressure: 6.07E-11mmHg at 25°C
• Melting Point: 218-220°C
• Refractive Index: 1.8240 (estimate)
• Boiling Point: 534°Cat760mmHg
• PKA: 4.71±0.30(Predicted)
• Flash Point: 240.3°C
• PSA: 12.89000
• Density: 1.274g/cm³
• LogP: 5.69440
• Storage Temp.: 2-8°C
• XLogP3: 6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 279.104799419
• Heavy Atom Count: 22
• Complexity: 369

Purity/Quality:

98%,99%, ^*data from raw suppliers

Dibenz[a,j]acridine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 40
• Safety Statements: 36/37

MSDS Files:

Total 1 MSDS from other Authors

Useful:

• Chemical Classes: Other Classes -> Polycyclic Aromatic Hydrocarbons
• Canonical SMILES: C1=CC=C2C(=C1)C=CC3=NC4=C(C=C32)C5=CC=CC=C5C=C4

Technology Process of Dibenz[a,j]acridine

There total 12 articles about Dibenz[a,j]acridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Dibenzo[a,j]acridine; compound with 4-fluoro-phenol → 4-Fluorophenol (371-41-5) + dibenz[a,j]acridine (224-42-0)

Guidance literature:

In tetrachloromethane; at 19.9 ℃; Thermodynamic data; Equilibrium constant;

DOI:10.1016/0584-8539(83)80131-7

Reference yield:

Dibenzo[a,j]acridine; compound with 3,4,5-trichloro-phenol → dibenz[a,j]acridine (224-42-0) + 3,4,5-trichlorophenol (609-19-8)

Guidance literature:

In tetrachloromethane; at 19.9 ℃; Thermodynamic data; Equilibrium constant;

DOI:10.1016/0584-8539(83)80131-7

Reference yield:

Dibenzo[a,j]acridine; compound with 2,2,2-trifluoro-ethanol → 2,2,2-trifluoroethanol (75-89-8) + dibenz[a,j]acridine (224-42-0)

Guidance literature:

In tetrachloromethane; at 19.9 ℃; Thermodynamic data; Equilibrium constant;

DOI:10.1016/0584-8539(83)80131-7

upstream raw materials:

1-<(2-Amino-1-naphthyl)methyl>-2-naphthol

1,4,10,13-tetrahydrodibenzacridine

1,4,8,9-tetrahydrodibenzacridine

formaldehyd

Downstream raw materials:

6-hydroxydibenzacridine

trans-3,4-dihydro-3,4-dihydroxydibenzacridine

trans-3,4-dihydroxy-1,2,3,4-tetrahydrodibenzacridine

7H-dibenzacridone

Refernces

• 1、 Juffernbruch, J.,Perkampus, H.-H.. "Untersuchungen zur H-Brueckenassoziation von Azaaromaten mit OH-Bruecken-II. H-Brueckenassoziationgleichgewichte von 1,2,7,8-Dibenzacridin mit verschiedenen OH-Donatoren: Ein Vergleich ir-Spektroskopischer und uv-vis-Spektroskopischer Messungen". . p. 1093 - 1096. Retrieved 2007/10/02.