C₂₂H₁₀F₂₆O₄

Base Information

• Chemical Name: C₂₂H₁₀F₂₆O₄
• CAS No.: 1420073-11-5
• Molecular Formula: C₂₂H₁₀F₂₆O₄
• Molecular Weight: 832.277
• Mol file: 1420073-11-5.mol

Synonyms:C₂₂H₁₀F₂₆O₄

Chemical Property of C₂₂H₁₀F₂₆O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₁₀F₂₆O₄

There total 2 articles about C₂₂H₁₀F₂₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1-carbomethoxy-3,5-dihydroxybenzene (2150-44-9) + 2,2,3,3,4,4,5,5,6,6,7,7,7-tridecafluoroheptyl trifluoromethanesulfonate → C22H10F26O4 (1420073-11-5)

Guidance literature:

1-carbomethoxy-3,5-dihydroxybenzene; With potassium carbonate; In N,N-dimethyl acetamide; at 90 ℃; Inert atmosphere;

2,2,3,3,4,4,5,5,6,6,7,7,7-tridecafluoroheptyl trifluoromethanesulfonate; In N,N-dimethyl acetamide; at 90 ℃; for 2h;

Reference yield:

2,2,3,3,4,4,5,5,6,6,7,7,7-tridecafluoroheptan-1-ol (375-82-6) → C22H10F26O4 (1420073-11-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 1 h / 20 °C / Cooling with ice

2.1: potassium carbonate / N,N-dimethyl acetamide / 90 °C / Inert atmosphere

2.2: 2 h / 90 °C

With potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl acetamide;

Reference yield: 76.0%

C22H10F26O4 (1420073-11-5) → C21H8F26O4 (1420073-12-6)

Guidance literature:

With water; potassium hydroxide; In ethanol; for 2h; Reflux;

upstream raw materials:

2,2,3,3,4,4,5,5,6,6,7,7,7-tridecafluoroheptan-1-ol

1-carbomethoxy-3,5-dihydroxybenzene

Downstream raw materials:

C₂₁H₈F₂₆O₄

Refernces