C₆₀H₅₉NO₁₀

Base Information

• Chemical Name: C₆₀H₅₉NO₁₀
• CAS No.: 1353094-10-6
• Molecular Formula: C₆₀H₅₉NO₁₀
• Molecular Weight: 954.129
• Mol file: 1353094-10-6.mol

Synonyms:C₆₀H₅₉NO₁₀

Chemical Property of C₆₀H₅₉NO₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₀H₅₉NO₁₀

There total 4 articles about C₆₀H₅₉NO₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

pyridine-2-carbaldehyde (1121-60-4) + 1,5-anhydro-2-deoxy-2-nitro-3,6-bis-O-(phenylmethyl)-4-O-[2,3,4,6-tetrakis-O-(phenylmethyl)-α-D-glucopyranosyl]-D-arabino-hex-1-enitol → C60H59NO10 (1353094-10-6)

Guidance literature:

With 3-benzyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazol-3-ium chloride; caesium carbonate; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ol202959y

Reference yield:

1,5-anhydro-2-deoxy-3,6-bis-O-(phenylmethyl)-4-O-[2,3,4,6-tetrakis-O-(phenylmethyl)-α-D-glucopyranosyl]-D-arabino-hex-1-enitol → C60H59NO10 (1353094-10-6)

Guidance literature:

Multi-step reaction with 2 steps

1: nitric acid; acetic anhydride / -33 - -10 °C / Inert atmosphere

2: 3-benzyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazol-3-ium chloride; caesium carbonate / dichloromethane / 24 h / 20 °C / Inert atmosphere

With nitric acid; 3-benzyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazol-3-ium chloride; acetic anhydride; caesium carbonate; In dichloromethane;

DOI:10.1021/ol202959y

Reference yield:

benzyl bromide (100-39-0) → C60H59NO10 (1353094-10-6)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 24 h / 20 °C / Inert atmosphere

2: nitric acid; acetic anhydride / -33 - -10 °C / Inert atmosphere

3: 3-benzyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazol-3-ium chloride; caesium carbonate / dichloromethane / 24 h / 20 °C / Inert atmosphere

With nitric acid; 3-benzyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazol-3-ium chloride; acetic anhydride; sodium hydride; caesium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;

DOI:10.1021/ol202959y

upstream raw materials:

pyridine-2-carbaldehyde

benzyl bromide

1,5-anhydro-2-deoxy-4-O-(α-D-glucopyranosyl)-D-arabino-hex-1-enitol

Refernces