C₁₄H₂₇NOS

Base Information

• Chemical Name: C₁₄H₂₇NOS
• CAS No.: 1018985-23-3
• Molecular Formula: C₁₄H₂₇NOS
• Molecular Weight: 257.44
• Mol file: 1018985-23-3.mol

Synonyms:C₁₄H₂₇NOS

Chemical Property of C₁₄H₂₇NOS

Chemical Property:

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Technology Process of C₁₄H₂₇NOS

There total 1 articles about C₁₄H₂₇NOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

heptane-2-thiol (628-00-2) + carbon dioxide (124-38-9,18923-20-1) + cyclohexylamine (108-91-8,157973-60-9) → C14H27NOS (1018985-23-3)

Guidance literature:

carbon dioxide; cyclohexylamine; In dimethyl sulfoxide; at 20 ℃; for 0.5h;

heptane-2-thiol; With triphenylphosphine; diethylazodicarboxylate; In dimethyl sulfoxide; at 20 ℃; for 4h; Further stages.;

DOI:10.1055/s-2008-1032025

upstream raw materials:

heptane-2-thiol

carbon dioxide

cyclohexylamine

Refernces