C₂₆H₂₄N₄O₄S₃

Base Information

• Chemical Name: C₂₆H₂₄N₄O₄S₃
• CAS No.: 1392144-30-7
• Molecular Formula: C₂₆H₂₄N₄O₄S₃
• Molecular Weight: 552.699
• Mol file: 1392144-30-7.mol

Synonyms:C₂₆H₂₄N₄O₄S₃

Chemical Property of C₂₆H₂₄N₄O₄S₃

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₂₆H₂₄N₄O₄S₃

There total 1 articles about C₂₆H₂₄N₄O₄S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-formylthiophene-2-boronic acid (17303-83-2) + ortho-bromobenzaldehyde (6630-33-7) → C26H24N4O4S3 (1392144-30-7)

Guidance literature:

Multi-step reaction with 2 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium fluoride dihydrate; tri tert-butylphosphoniumtetrafluoroborate / tetrahydrofuran / Inert atmosphere

2: methanol / 0.17 h / 60 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium fluoride dihydrate; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; methanol; 1: Suzuki-Miyaura coupling;

DOI:10.1002/anie.201201374

Reference yield: 90.0%

C26H24N4O4S3 (1392144-30-7) → naphtho[1,2-b]thiophene (234-41-3)

Guidance literature:

With dirhodium tetraacetate; lithium tert-butoxide; In toluene; at 90 ℃; for 1h; Inert atmosphere; Molecular sieve;

DOI:10.1002/anie.201201374

upstream raw materials:

3-formylthiophene-2-boronic acid

ortho-bromobenzaldehyde

Downstream raw materials:

naphtho[1,2-b]thiophene

Refernces