2,4-diiodochlorobenzene

Base Information

• Chemical Name: 2,4-diiodochlorobenzene
• CAS No.: 31928-48-0
• Molecular Formula: C₆H₃ClI₂
• Molecular Weight: 364.352
• Mol file: 31928-48-0.mol

Synonyms:2,4-diiodochlorobenzene

Chemical Property of 2,4-diiodochlorobenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-diiodochlorobenzene

There total 2 articles about 2,4-diiodochlorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-Chloro-4-iodobenzene (637-87-6) → 2,4-diiodochlorobenzene (31928-48-0)

Guidance literature:

1-Chloro-4-iodobenzene; With Li(2,2,6,6-tetramethylpiperidide)*Al(ⁱBu)₃; In tetrahydrofuran; hexane; at -78 ℃; for 3h;

With iodine; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 1h;

DOI:10.1021/ja064601n

Reference yield:

chlorobenzene (108-90-7) → 2,4-diiodochlorobenzene (31928-48-0)

Guidance literature:

With sulfuric acid; iodine;

Reference yield:

2,4-diiodochlorobenzene (31928-48-0) + (trifluoromethyl)trimethylsilane (81290-20-2) → 4-chloro-α,α,α,α',α',α'-hexafluoro-m-xylene (327-76-4)

Guidance literature:

With potassium fluoride; copper(l) iodide; 1,10-Phenanthroline; Trimethyl borate; In dimethyl sulfoxide; at 60 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ol501967c

upstream raw materials:

chlorobenzene

1-Chloro-4-iodobenzene

Downstream raw materials:

4-chloro-α,α,α,α',α',α'-hexafluoro-m-xylene

Refernces