(4-Nitrophenyl)azanium;chloride

Base Information

• Chemical Name: (4-Nitrophenyl)azanium;chloride
• CAS No.: 15873-51-5
• Molecular Formula: C6H6 N2 O2 . Cl H
• Molecular Weight: 174.587
• Mol file: 15873-51-5.mol

Synonyms:(4-nitrophenyl)azanium;chloride

Chemical Property of (4-Nitrophenyl)azanium;chloride

Chemical Property:

• Melting Point: 145-146 °C
• Boiling Point: 211.6°Cat760mmHg
• Flash Point: 84.2°C
• PSA: 71.84000
• Density: 0.94g/cm³
• LogP: 3.08340
• Storage Temp.: Sealed in dry,Room Temperature
• Solubility.: soluble in Methanol
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 174.0196052
• Heavy Atom Count: 11
• Complexity: 129

Purity/Quality:

98%,99%, ^*data from raw suppliers

4-Nitroaniline Hydrochloride ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1[NH3+])[N+](=O)[O-].[Cl-]

Technology Process of (4-Nitrophenyl)azanium;chloride

There total 9 articles about (4-Nitrophenyl)azanium;chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.8%

N-(4-Nitrophenyl)acetamide (104-04-1) → 4-nitroaniline hydrochloride (15873-51-5)

Guidance literature:

With thionyl chloride; In methanol; for 0.1h; Reflux;

DOI:10.1007/s11164-011-0327-6

Reference yield: 99.8%

2-chloro-N-(4-nitro-phenyl)-acetamide (17329-87-2) → 4-nitroaniline hydrochloride (15873-51-5)

Guidance literature:

With thionyl chloride; In methanol; for 0.05h; Reflux;

DOI:10.1007/s11164-011-0327-6

Reference yield: 96.0%

C21H16N2O5 → 1,3-diphenyl-propane-1,2,3-trione (643-75-4) + 4-nitroaniline hydrochloride (15873-51-5)

Guidance literature:

With hydrogenchloride; In dichloromethane; water; at 20 ℃;

DOI:10.1016/j.tet.2016.03.093

upstream raw materials:

N-(4-nitrophenyl)-4-methylbenzenesulfonamide

aniline hydrochloride

(2-Methoxy-6-{[(E)-4-nitro-phenylimino]-methyl}-8,9-dihydro-7H-benzocyclohepten-5-yl)-(4-nitro-phenyl)-amine; hydrochloride

4-nitro-aniline

Downstream raw materials:

6-methoxy-3,4-dihydro-2H-quinoline-1-carbonimidic acid-(4-nitro-anilide)

2-nitro-3-(4-nitro-anilino)-acrylaldehyde

3-(4-nitro-anilino)-crotonic acid-(4-nitro-anilide)

5-(4-nitrophenyl)-2-furaldehyde

Refernces

• 1、 Adardour, Mohamed,Boutafda, Aziz,Hdoufane, Ismail,Aghraz, Abdellah,Hafidi, Mohamed,Zaballos-García, Elena,Cherqaoui, Driss,Baouid, Abdesselam. "Efficient and simple synthesis of novel 1,2,3-triazolyl-linked benzimidazolone, molecular docking and evaluation of their antimicrobial activity". . p. 3490 - 3506. Retrieved 2020/08/19.
• 2、 Yuki, Tatsuya,Yonekawa, Morio,Furusho, Yoshio,Sei, Yoshihisa,Tomita, Ikuyoshi,Endo, Takeshi. "Reversible capture and release of aromatic amines by vicinal tricarbonyl compound". . p. 2868 - 2873. Retrieved 2016/05/19.