Technology Process of C28H27NO
There total 4 articles about C28H27NO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(methoxymethyl)triphenylphosphonium chloride;
With
potassium tert-butylate;
In
tetrahydrofuran; diethyl ether;
at 20 ℃;
for 0.5h;
C26H23NO;
In
tetrahydrofuran; diethyl ether;
at 20 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: bis(dibenzylideneacetone)-palladium(0); dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate / toluene; water / 5 h / 130 °C
2.1: potassium tert-butylate / diethyl ether; tetrahydrofuran / 0.5 h / 20 °C
2.2: 16 h / 20 °C
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; potassium tert-butylate; bis(dibenzylideneacetone)-palladium(0);
In
tetrahydrofuran; diethyl ether; water; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 6 h / 60 °C / Inert atmosphere
2.1: bis(dibenzylideneacetone)-palladium(0); dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate / toluene; water / 5 h / 130 °C
3.1: potassium tert-butylate / diethyl ether; tetrahydrofuran / 0.5 h / 20 °C
3.2: 16 h / 20 °C
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tetrakis(triphenylphosphine) palladium(0); potassium tert-butylate; sodium carbonate; bis(dibenzylideneacetone)-palladium(0);
In
tetrahydrofuran; diethyl ether; ethanol; water; toluene;