2-ClC₆H₄CH₂OBn

Base Information

• Chemical Name: 2-ClC₆H₄CH₂OBn
• CAS No.: 52322-07-3
• Molecular Formula: C₁₄H₁₃ClO
• Molecular Weight: 232.71
• Mol file: 52322-07-3.mol

Synonyms:2-ClC₆H₄CH₂OBn

Chemical Property of 2-ClC₆H₄CH₂OBn

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-ClC₆H₄CH₂OBn

There total 2 articles about 2-ClC₆H₄CH₂OBn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2-Chlorobenzyl alcohol (17849-38-6) + benzyl chloride (100-44-7) → 2-ClC6H4CH2OBn (52322-07-3)

Guidance literature:

With iron(III) perchlorate; at 100 ℃; for 1h; neat (no solvent);

DOI:10.1007/s00706-008-0054-x

Reference yield:

1-bromomethyl-2-chlorobenzene (611-17-6) → 2-ClC6H4CH2OBn (52322-07-3)

Guidance literature:

With benzyl alcohol; at 120 ℃;

DOI:10.1039/jr9590003183

Reference yield:

phosgene (75-44-5) + diethyl ether (60-29-7,927820-24-4) + 2-ClC6H4CH2OBn (52322-07-3) + isopropylmagnesium bromide (920-39-8) → 2-Chlorobenzyl alcohol (17849-38-6) + toluene (108-88-3,15644-74-3,16713-13-6) + benzyl alcohol (100-51-6,185532-71-2)

Guidance literature:

DOI:10.1039/jr9590003183

upstream raw materials:

1-bromomethyl-2-chlorobenzene

2-Chlorobenzyl alcohol

benzyl chloride

Downstream raw materials:

2-Chlorobenzyl alcohol

toluene

benzyl alcohol

Refernces