1-(4-Decylphenyl)ethanone

Base Information

• Chemical Name: 1-(4-Decylphenyl)ethanone
• CAS No.: 37593-06-9
• Molecular Formula: C18H28O
• Molecular Weight: 260.42
• Hs Code.: 2914399090
• NSC Number: 39801
• DSSTox Substance ID: DTXSID70958645
• Wikidata: Q82939171
• Mol file: 37593-06-9.mol

Synonyms:1-(4-decylphenyl)ethanone;1-(4-decylphenyl)ethan-1-one;37593-06-9;NSC39801;Maybridge1_002045;4'-(Dec-1-yl)acetophenone;SCHEMBL9997622;HMS547E21;DTXSID70958645;MFCD00173754;NSC-39801;AKOS024349855;CS-0357829;FT-0605704;A823784

Chemical Property of 1-(4-Decylphenyl)ethanone

Chemical Property:

• Vapor Pressure: 1.04E-05mmHg at 25°C
• Melting Point: 33 °C
• Refractive Index: 1.491
• Boiling Point: 371.4 °C at 760 mmHg
• Flash Point: 156.6 °C
• PSA: 17.07000
• Density: 0.911 g/cm³
• LogP: 5.57240
• XLogP3: 6.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 10
• Exact Mass: 260.214015512
• Heavy Atom Count: 19
• Complexity: 226

Purity/Quality:

98%min ^*data from raw suppliers

4'-(Dec-1-yl)acetophenone ^*data from reagent suppliers

Safty Information:

• Safety Statements: S24/25:Avoid contact with skin and eyes.

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCC1=CC=C(C=C1)C(=O)C

Technology Process of 1-(4-Decylphenyl)ethanone

There total 4 articles about 1-(4-Decylphenyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

decylbenzene (104-72-3) + acetyl chloride (75-36-5) → n-decyl-4' acetophenone (37593-06-9)

Guidance literature:

aluminium trichloride; In carbon disulfide; 0 deg C, 1 h, RT, 2 h;

Reference yield:

decylbenzene (104-72-3) + acetic anhydride (108-24-7) → n-decyl-4' acetophenone (37593-06-9)

Guidance literature:

With aluminium trichloride; In dichloromethane; at 20 ℃; for 5h;

DOI:10.1021/ma035947a

Reference yield:

2-(4-Decyl-phenyl)-2-methyl-[1,3]dithiane (107678-20-6) → n-decyl-4' acetophenone (37593-06-9)

Guidance literature:

With methyltriphenylphosphonium tribromide; water; Yield given. Multistep reaction; 1.) THF, 3 h, room temperature;

DOI:10.1016/S0040-4039(00)84691-2

upstream raw materials:

decylbenzene

acetyl chloride

2-(4-Decyl-phenyl)-2-methyl-[1,3]dithiane

acetic anhydride

Downstream raw materials:

4-n-decyl-α-bromoacetophenone

4-decyl-3-nitro-benzoic acid

Potassium; 2-[2-(4-decyl-phenyl)-1-hydroxy-2-oxo-ethyl]-3-oxo-hexanoate

1-(4-Decyl-phenyl)-2-hydroxy-heptane-1,4-dione

Refernces

• 1、 Krati, Noureddine,Roizard, Denis,Brembilla, Alain,Lochon, Pierre. "Nouveaux diamino-3,4 phenylalcanes et leur transformation en benzimidazolemethanethiols-2". . p. 443 - 448. Retrieved 2007/10/02.
• 2、 Liang, Jason. "The Synthesis of 3-Aryl-6-alkylpyridazines". . p. 1297 - 1299. Retrieved 2007/10/02.