1,3-DIMETHYLTRIAZENE

Base Information

• Chemical Name: 1,3-DIMETHYLTRIAZENE
• CAS No.: 3585-32-8
• Molecular Formula: C₂H₇N₃
• Molecular Weight: 73.0977
• Mol file: 3585-32-8.mol

Synonyms:Triazene,1,3-dimethyl- (7CI,8CI); 1,3-Dimethyltriazene

Chemical Property of 1,3-DIMETHYLTRIAZENE

Chemical Property:

• Vapor Pressure: 282mmHg at 25°C
• Refractive Index: 1.4854 (estimate)
• Boiling Point: 50.8°C at 760 mmHg
• PSA: 36.75000
• Density: 0.95g/cm³
• LogP: 0.59370

Purity/Quality:

99% ^*data from raw suppliers

1,3-DIMETHYLTRIAZENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-DIMETHYLTRIAZENE

There total 2 articles about 1,3-DIMETHYLTRIAZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C4H10N4O (103711-40-6) → methanol (67-56-1) + methylphosphate (812-00-0) + N,N'-Dimethylurea (96-31-1) + 1,3-Dimethyltriazene (3585-32-8,115246-94-1,115246-96-3,467426-36-4) + methylamine (74-89-5)

Guidance literature:

With 2,6-diaminocaproic acid; sodium perchlorate; In acetonitrile; at 70 ℃; Rate constant; variation of pH, solvent deuterium isotope effect;

DOI:10.1021/jo00050a016

Reference yield:

C5H11N3O2 (88211-12-5) → ethanol (64-17-5) + 1,3-Dimethyltriazene (3585-32-8,115246-94-1,115246-96-3,467426-36-4)

Guidance literature:

With lysine buffer; sodium perchlorate; In acetonitrile; at 70 ℃; Rate constant; variation of pH, solvent deuterium isotope effect;

DOI:10.1021/jo00050a016

Reference yield: 77.0%

1,3-dimethyl-1-triazene (3585-32-8,115246-94-1,115246-96-3,467426-36-4) + methyl isocyanate (624-83-9) → 1,3-dimethyl-3-(N-methylcarbamoyl)triazene (103711-40-6)

Guidance literature:

In pentane; Heating;

DOI:10.1021/jo00370a002

upstream raw materials:

C₄H₁₀N₄O

C₅H₁₁N₃O₂

Downstream raw materials:

methylamine

methanol

<2H1>methan<2H>ol

deuteromethanol

Refernces