5,5'-diethynyl-2,2'-bipyrimidine

Base Information

• Chemical Name: 5,5'-diethynyl-2,2'-bipyrimidine
• CAS No.: 718606-37-2
• Molecular Formula: C₄₂H₂₄N₁₀
• Molecular Weight: 668.72
• Mol file: 718606-37-2.mol

Synonyms:5,5'-diethynyl-2,2'-bipyrimidine

Chemical Property of 5,5'-diethynyl-2,2'-bipyrimidine

Chemical Property:

Purity/Quality:

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Technology Process of 5,5'-diethynyl-2,2'-bipyrimidine

There total 1 articles about 5,5'-diethynyl-2,2'-bipyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

4'-{[(Trifluoromethyl)sulfonyl]oxy}-2,2':6',2''-terpyridine (134653-69-3) + 5,5'-diethynyl-2,2'-bipyrimidine (679844-18-9) → 5,5'-diethynyl-2,2'-bipyrimidine (718606-37-2)

Guidance literature:

With diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; at 80 ℃;

DOI:10.1016/j.tetlet.2004.03.147

upstream raw materials:

4'-{[(Trifluoromethyl)sulfonyl]oxy}-2,2':6',2''-terpyridine

5,5'-diethynyl-2,2'-bipyrimidine

Refernces