1-benzoyl-3-phenylsulfonylazulene

Base Information

• Chemical Name: 1-benzoyl-3-phenylsulfonylazulene
• CAS No.: 78049-23-7
• Molecular Formula: C₂₃H₁₆O₃S
• Molecular Weight: 372.444
• Mol file: 78049-23-7.mol

Synonyms:1-benzoyl-3-phenylsulfonylazulene

Chemical Property of 1-benzoyl-3-phenylsulfonylazulene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-benzoyl-3-phenylsulfonylazulene

There total 5 articles about 1-benzoyl-3-phenylsulfonylazulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.5%

1-bromo-3-benzoylazulene (78049-20-4) → 1-benzoyl-3-phenylsulfonylazulene (78049-23-7)

Guidance literature:

In acetone; at 72 ℃; for 0.0833333h;

Reference yield:

1,3-diiodoazulene (36044-42-5) → 1-benzoyl-3-phenylsulfonylazulene (78049-23-7)

Guidance literature:

Multi-step reaction with 4 steps

1: 92 percent / cupric bromide / acetonitrile / 20 °C

2: 3 percent / copper (powder) / decane / 0.33 h / 100 °C

3: 98 percent / cupric bromide / acetonitrile

4: 78.5 percent / acetone / 0.08 h / 72 °C

With copper; copper(ll) bromide; In decane; acetone; acetonitrile;

Reference yield:

1,3-dibromoazulene (14658-95-8) → 1-benzoyl-3-phenylsulfonylazulene (78049-23-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 3 percent / copper (powder) / decane / 0.33 h / 100 °C

2: 98 percent / cupric bromide / acetonitrile

3: 78.5 percent / acetone / 0.08 h / 72 °C

With copper; copper(ll) bromide; In decane; acetone; acetonitrile;

upstream raw materials:

1-bromo-3-benzoylazulene

1,3-diiodoazulene

1,3-dibromoazulene

azulen-1-yl(phenyl)methanone

Refernces