Technology Process of C21H18ClN7O10S4
There total 6 articles about C21H18ClN7O10S4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
water; acetonitrile;
at 40 ℃;
pH=5 - 7;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: lithium carbonate / dimethyl sulfoxide / 1 h / 35 °C
1.2: 58 °C
2.1: dihydrogen peroxide / sodium tungstate (VI) dihydrate / water; acetic acid / 30 - 60 °C
3.1: trichlorophosphate / acetonitrile; ISOPROPYLAMIDE / 2 h / 45 - 60 °C
4.1: acetonitrile; water / 2.83 h / 5 °C
5.1: sodium hydroxide / acetone / 2 h / 0 °C / pH 6
6.1: acetonitrile; water / 40 °C / pH 5 - 7
With
dihydrogen peroxide; lithium carbonate; sodium hydroxide; trichlorophosphate;
sodium tungstate (VI) dihydrate;
In
ISOPROPYLAMIDE; water; acetic acid; dimethyl sulfoxide; acetone; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dihydrogen peroxide / sodium tungstate (VI) dihydrate / water; acetic acid / 30 - 60 °C
2: trichlorophosphate / acetonitrile; ISOPROPYLAMIDE / 2 h / 45 - 60 °C
3: acetonitrile; water / 2.83 h / 5 °C
4: sodium hydroxide / acetone / 2 h / 0 °C / pH 6
5: acetonitrile; water / 40 °C / pH 5 - 7
With
dihydrogen peroxide; sodium hydroxide; trichlorophosphate;
sodium tungstate (VI) dihydrate;
In
ISOPROPYLAMIDE; water; acetic acid; acetone; acetonitrile;