diethyl 2-bromoadipate

Base Information

• Chemical Name: diethyl 2-bromoadipate
• CAS No.: 7209-01-0
• Molecular Formula: C₁₀H₁₇BrO₄
• Molecular Weight: 281.147
• Mol file: 7209-01-0.mol

Synonyms:diethyl 2-bromoadipate

Chemical Property of diethyl 2-bromoadipate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of diethyl 2-bromoadipate

There total 1 articles about diethyl 2-bromoadipate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

diethyl 2,5-dibromoadipate (869-10-3) → diethyl adipate (141-28-6) + diethyl 2-bromoadipate (7209-01-0)

Guidance literature:

With DMBI; In tetrahydrofuran; for 6h; Heating;

DOI:10.1021/jo00376a064

Reference yield:

tetrachloromethane (56-23-5) + diethyl 2-bromoadipate (7209-01-0) → 2-ethoxycarbonyl-1-cyclopentanone (611-10-9)

Guidance literature:

unter Kuehlung; anschliessendes Behandeln mit verd.Salzsaeure;

Reference yield:

diethyl 2-bromoadipate (7209-01-0) → 2-ethoxycarbonyl-1-cyclopentanone (611-10-9)

Guidance literature:

Multi-step reaction with 3 steps

1: methanol / beim Behandeln des Reaktionsprodukts mit Aethanol und wenig Schwefelsaeure

2: sulfuric acid / beim anschliessenden Behandeln mit Wasser

3: sodium ethylate; ethanol

With methanol; ethanol; sulfuric acid; sodium ethanolate;

upstream raw materials:

diethyl 2,5-dibromoadipate

Downstream raw materials:

2-Phenoxy-adipinsaeure-diaethylester

α-<1-Hydroxy-cyclohexyl>-adipinsaeure-diethylester

1,4-Bis-ethoxycarbonyl-butan-1-phosphonsaeure-diethylester

2-hydroxyadipic acid

Refernces