(1S,2R,3S)-3-hydroxycyclohex-4-ene-1,2-dicarbonyl diazide

Base Information

• Chemical Name: (1S,2R,3S)-3-hydroxycyclohex-4-ene-1,2-dicarbonyl diazide
• CAS No.: 1018454-69-7
• Molecular Formula: C₈H₈N₆O₃
• Molecular Weight: 236.19
• Mol file: 1018454-69-7.mol

Synonyms:(1S,2R,3S)-3-hydroxycyclohex-4-ene-1,2-dicarbonyl diazide

Chemical Property of (1S,2R,3S)-3-hydroxycyclohex-4-ene-1,2-dicarbonyl diazide

Chemical Property:

Purity/Quality:

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Technology Process of (1S,2R,3S)-3-hydroxycyclohex-4-ene-1,2-dicarbonyl diazide

There total 1 articles about (1S,2R,3S)-3-hydroxycyclohex-4-ene-1,2-dicarbonyl diazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(trimethylsiloxy)-1,3-butadiene (6651-43-0) + dimethylfumarate (624-49-7) → (1S,2R,3S)-3-hydroxycyclohex-4-ene-1,2-dicarbonyl diazide (1018454-69-7)

Guidance literature:

1-(trimethylsiloxy)-1,3-butadiene; dimethylfumarate; With (1S,2S,6R)-2-diphenylphosphinyl-6-(4,5-difluoro-2-phenoxy)cyclohexanol; barium isopropoxide; cesium fluoride; In tetrahydrofuran; at -20 ℃; for 96h; Inert atmosphere;

With hydrogenchloride; In water; Further stages;

DOI:10.1002/anie.200804777

upstream raw materials:

1-(trimethylsiloxy)-1,3-butadiene

dimethylfumarate

Refernces