1-(4-(methyl-d3)phenyl)ethan-1-one

Base Information Edit

Chemical Name:1-(4-(methyl-d3)phenyl)ethan-1-one
CAS No.:114379-92-9
Molecular Formula:C₉H₁₀O
Molecular Weight:137.154
Hs Code.:
Mol file:114379-92-9.mol

Synonyms:1-(4-(methyl-d3)phenyl)ethan-1-one

Suppliers and Price of 1-(4-(methyl-d3)phenyl)ethan-1-one

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-(methyl-d3)phenyl)ethan-1-one Edit

Chemical Property:

Purity/Quality:: 96% ^*data from raw suppliers

Safty Information:

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Useful:

Uses 4''-Methyl-d3-acetophenone is used in preparation of crystalline forms of substituted Imidazopyrazinecarboxamides as Phosphoinositide 3-kinase (PI3K) inhibitors. I is the labeled form of 4''-Methylacetophenone(M275305); 4''-Methylacetophenone is a methylated acteophenone used in cosmetics and perfumery. The presence of 4''-Methylacetophenone has been shown to accelerate the photopolymerization of Methyl methacrylate.

Technology Process of 1-(4-(methyl-d3)phenyl)ethan-1-one

There total 5 articles about 1-(4-(methyl-d3)phenyl)ethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.3%

: 865-50-9
iodomethane-d3

: 149104-90-5
4-acetylphenylboronic acid

: 114379-92-9
1-(4-(methyl-d3)phenyl)ethan-1-one

Guidance literature:: With bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); cesium fluoride; In water; N,N-dimethyl-formamide; at 45 ℃; Inert atmosphere;

Reference yield: 62.0%

: 13329-40-3
4-Iodoacetophenone

: 7575-93-1
methyl-d3 4-methylbenzenesulfonate

: 114379-92-9
1-(4-(methyl-d3)phenyl)ethan-1-one

Guidance literature:: With manganese; chloro-trimethyl-silane; salcomine; bis(bipyridine)nickel(II) bromide; In N,N-dimethyl-formamide; at 30 ℃; for 24h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01863