Technology Process of 2-bromo-4-methoxy-6-pentylaniline
There total 7 articles about 2-bromo-4-methoxy-6-pentylaniline which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hypophosphorous acid;
palladium on activated charcoal;
In
methanol;
for 0.5h;
Heating;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1.) Mg / 1.) ether, 2.) ether, a) RT, 1 h, b) reflux, 10 min
2: 92 percent / H2, conc. aq. HCl / 10percent Pd/C / acetic acid
3: 71 percent / Br2, Al / 0.25 h / Ambient temperature
4: 93 percent / AlCl3 / benzene / 0.25 h / Heating
5: 30 percent / 70percent HNO3, AcOH / 0.5 h / 10 - 12 °C
6: K2CO3 / dimethylformamide / Ambient temperature
7: 81 percent / 50percent phosphinic acid / 10percent Pd/C / methanol / 0.5 h / Heating
With
hydrogenchloride; aluminium trichloride; hydrogen; bromine; nitric acid; hypophosphorous acid; potassium carbonate; magnesium; acetic acid; aluminium;
palladium on activated charcoal;
In
methanol; acetic acid; N,N-dimethyl-formamide; benzene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 71 percent / Br2, Al / 0.25 h / Ambient temperature
2: 93 percent / AlCl3 / benzene / 0.25 h / Heating
3: 30 percent / 70percent HNO3, AcOH / 0.5 h / 10 - 12 °C
4: K2CO3 / dimethylformamide / Ambient temperature
5: 81 percent / 50percent phosphinic acid / 10percent Pd/C / methanol / 0.5 h / Heating
With
aluminium trichloride; bromine; nitric acid; hypophosphorous acid; potassium carbonate; acetic acid; aluminium;
palladium on activated charcoal;
In
methanol; N,N-dimethyl-formamide; benzene;
