2-TETRAHYDROFURFURYL ISOTHIOCYANATE

Base Information

• Chemical Name: 2-TETRAHYDROFURFURYL ISOTHIOCYANATE
• CAS No.: 36810-87-4
• Molecular Formula: C6H9NOS
• Molecular Weight: 143.21
• Hs Code.: 38220090
• Mol file: 36810-87-4.mol

Synonyms:Isothiocyanicacid, tetrahydrofurfuryl ester (6CI);2-(Isothiocyanatomethyl)tetrahydrofuran;2-Tetrahydrofuranylmethyl isothiocyanate;2-Tetrahydrofurfuryl isothiocyanate;2-Tetrahydrofurylmethyl isothiocyanate;CHE 8570;Tetrahydro-2-(isothiocyanatomethyl)furan;Tetrahydrofuran-2-methylisothiocyanate;Tetrahydrofurfuryl isothiocyanate;

Chemical Property of 2-TETRAHYDROFURFURYL ISOTHIOCYANATE

Chemical Property:

• Vapor Pressure: 0.0288mmHg at 25°C
• Refractive Index: 1.5350
• Boiling Point: 253.7 °C at 760 mmHg
• Flash Point: 107.2 °C
• PSA: 53.68000
• Density: 1.19 g/cm³
• LogP: 1.26820
• Sensitive.: Moisture Sensitive/Lachrymatory

Purity/Quality:

98%min ^*data from raw suppliers

2-(isothiocyanatomethyl)tetrahydrofuran ^*data from reagent suppliers

Safty Information:

• Pictogram(s): C,Xi
• Hazard Codes: C,Xi
• Statements: 20/21/22-36/37/38-34
• Safety Statements: 26-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-TETRAHYDROFURFURYL ISOTHIOCYANATE

There total 4 articles about 2-TETRAHYDROFURFURYL ISOTHIOCYANATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C9H15NO3S2 → tetrahydrofurfuryl isothiocyanate (36810-87-4)

Guidance literature:

With triethylamine; In 1,4-dioxane; chloroform; at 20 ℃; for 0.0833333h;

DOI:10.1007/s11243-010-9375-9

Reference yield:

TETRAHYDROFURFURYLAMINE (4795-29-3) → tetrahydrofurfuryl isothiocyanate (36810-87-4)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / 1,4-dioxane / -10 - 20 °C

2: 1,4-dioxane / -10 °C

3: triethylamine / 1,4-dioxane; chloroform / 0.08 h / 20 °C

With triethylamine; In 1,4-dioxane; chloroform;

DOI:10.1007/s11243-010-9375-9

Reference yield:

C6H11NOS2 (847253-26-3) → tetrahydrofurfuryl isothiocyanate (36810-87-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 1,4-dioxane / -10 °C

2: triethylamine / 1,4-dioxane; chloroform / 0.08 h / 20 °C

With triethylamine; In 1,4-dioxane; chloroform;

DOI:10.1007/s11243-010-9375-9

upstream raw materials:

TETRAHYDROFURFURYLAMINE

carbon disulfide

C₆H₁₁NOS₂

Downstream raw materials:

1-((tetrahydrofuran-2-yl)methyl)thiourea

2-benzyl-4-(tetrahydro-furan-2-ylmethyl)-[1,2,4]thiadiazolidine-3,5-dione

4-(2-furylmethyl)thiosemicarbazide

Refernces