{(η5-cyclopentadienyl)W(CO)3}2PbEt2

Base Information

• Chemical Name: {(η5-cyclopentadienyl)W(CO)3}2PbEt2
• CAS No.: 79123-28-7
• Molecular Formula: C₂₀H₂₀O₆PbW₂
• Molecular Weight: 931.275
• Mol file: 79123-28-7.mol

Synonyms:{(η5-cyclopentadienyl)W(CO)3}2PbEt2

Chemical Property of {(η5-cyclopentadienyl)W(CO)3}2PbEt2

Chemical Property:

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Technology Process of {(η5-cyclopentadienyl)W(CO)3}2PbEt2

There total 1 articles about {(η5-cyclopentadienyl)W(CO)3}2PbEt2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

(η5-cyclopentadienyl)W(CO)3PbEt3 (79110-50-2) → {(η5-cyclopentadienyl)W(CO)3}2PbEt2 (79123-28-7) + tetraethyllead(IV) (78-00-2)

Guidance literature:

heated in vac. to 60°C for 8 h, under nitrogen, yellow-orange liquid became solid and darker orange in colour; dissolved in CH2Cl2/hexane solution, placed upon alumina column, elutedwith hexane, then hexane/CH2Cl2 solution, concentrated and placed refrigerator;

DOI:10.1016/S0022-328X(00)85955-0

upstream raw materials:

(η5-cyclopentadienyl)W(CO)3PbEt3

Refernces