Technology Process of C13H13FN2O2
There total 6 articles about C13H13FN2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; sodium hydroxide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 20 °C / Cooling with ice
2.1: manganese(IV) oxide / tetrahydrofuran / 3 h / 70 °C
3.1: sodium hydride / tetrahydrofuran / 0.25 h / Cooling with ice
3.2: 2 h / 20 °C / Cooling with ice
4.1: hydrogen / palladium 10% on activated carbon / ethanol; tetrahydrofuran / 20 h / 20 °C
5.1: sodium hydroxide; water
With
manganese(IV) oxide; lithium aluminium tetrahydride; water; hydrogen; sodium hydride; sodium hydroxide;
palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 2 h / 120 °C
1.2: 2.5 h / 80 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 20 °C / Cooling with ice
3.1: manganese(IV) oxide / tetrahydrofuran / 3 h / 70 °C
4.1: sodium hydride / tetrahydrofuran / 0.25 h / Cooling with ice
4.2: 2 h / 20 °C / Cooling with ice
5.1: hydrogen / palladium 10% on activated carbon / ethanol; tetrahydrofuran / 20 h / 20 °C
6.1: sodium hydroxide; water
With
manganese(IV) oxide; lithium aluminium tetrahydride; water; hydrogen; sodium hydride; sodium hydroxide;
palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol;
