[(C₅H₅)2TiSe₂C₂(CO₂CH₃)2]

Base Information Edit

Chemical Name:[(C₅H₅)2TiSe₂C₂(CO₂CH₃)2]
CAS No.:82865-10-9
Molecular Formula:C₁₆H₁₆O₄Se₂Ti
Molecular Weight:478.101
Hs Code.:
Mol file:82865-10-9.mol

[(C<sub>5</sub>H<sub>5</sub>)2TiSe<sub>2</sub>C<sub>2</sub>(CO<sub>2</sub>CH<sub>3</sub>)2]

Synonyms:[(C₅H₅)2TiSe₂C₂(CO₂CH₃)2]

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Chemical Property of [(C₅H₅)2TiSe₂C₂(CO₂CH₃)2] Edit

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Technology Process of [(C₅H₅)2TiSe₂C₂(CO₂CH₃)2]

There total 1 articles about [(C₅H₅)2TiSe₂C₂(CO₂CH₃)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 12307-22-1
titanocene pentaselenide

: 762-42-5
dimethyl acetylenedicarboxylate

: 7782-49-2
selenium

: 82865-10-9
[(C₅H₅)2TiSe₂C₂(CO₂CH₃)2]

Guidance literature:: In xylene; under N2, xylene soln. of Ti complex and dimethyl acetylenedicarboxylate refluxed for 0.5 h; cooled, filtered, Se washed with CH2Cl2, filtrate evapd. to oil, dissolved in small amt. of CH2Cl2, chromd., diluted with CH2Cl2, concd. in vac., cooled at -20°C, filtered;

Reference yield: 93.0%

: 82865-10-9
[(C₅H₅)2TiSe₂C₂(CO₂CH₃)2]

: 15629-92-2
[NiCl₂((C₆H₅)2PC₃H₆P(C₆H₅)2)]*CH₂Cl₂

: 82865-15-4
[Ni(Se₂C₂(CO₂CH₃)2)((C₆H₅)2PC₃H₆P(C₆H₅)2)]

Guidance literature:: In dichloromethane; under N2, soln. of Ni complex and Ti complex in CH2Cl2 stirred for 5 min at room temp.; evapd. to dryness, dissolved in min. amt. of CH2Cl2, chromd., added ether, filtered;

Reference yield: 93.0%

: 10199-34-5,14056-88-3,15604-36-1
cis-dichlorobis(triphenylphosphine)platinum(II)

: 82865-10-9
[(C₅H₅)2TiSe₂C₂(CO₂CH₃)2]

: 124-41-4
sodium methylate

: 82865-13-2
[Pt(Se₂C₂(CO₂CH₃)2)(P(C₆H₅)3)2]

Guidance literature:: In methanol; under N2, NaOCH3 added to slurry of Ti complex in methanol, to purple soln. added Pt complex, stirred for 10 min; slurry concd., filtered, residue washed with methanol, extd. with CH2Cl2, extract diluted with methanol, concd., filtered;