Technology Process of [1,1'-Biphenyl]-4-sulfonic acid
There total 6 articles about [1,1'-Biphenyl]-4-sulfonic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate; Aminoiminomethanesulfinic acid;
In
dimethyl sulfoxide;
at 100 ℃;
for 14h;
Green chemistry;
DOI:10.1039/d0gc03135f
- Guidance literature:
-
With
chlorosulfonic acid;
In
chloroform;
for 1.5h;
Inert atmosphere;
Cooling with ice;
DOI:10.1002/ardp.201600251
- Guidance literature:
-
phenylboronic acid; 4-iodobenzenesulfonate-functionalized Argogel-MBOH resin;
With
potassium carbonate;
tris-(dibenzylideneacetone)dipalladium(0);
In
dichloromethane; N,N-dimethyl-formamide;
Heating;
With
trifluoroacetic acid;
In
dichloromethane;
for 1h;
Further stages.;
DOI:10.1021/ol991163z