difluoro(dimethyl)germane

Base Information

• Chemical Name: difluoro(dimethyl)germane
• CAS No.: 811-70-1
• Molecular Formula: C₂H₆F₂Ge
• Molecular Weight: 140.656
• Mol file: 811-70-1.mol

Synonyms:

Chemical Property of difluoro(dimethyl)germane

Chemical Property:

• Vapor Pressure: 1280mmHg at 25°C
• Boiling Point: 10.1°C at 760 mmHg

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of difluoro(dimethyl)germane

There total 2 articles about difluoro(dimethyl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

ammonium fluoride + phenylgermasesquioxane → Dimethylgermanium-difluorid (811-70-1)

Guidance literature:

With sulfuric acid; to ice cooled Ge compd. added concd. H2SO4 dropwise with stirring for 1 h, then added solid NH4F, stirred at room temp. for 1 h; shaked with CH2Cl2, org. phase neutralised with K2CO3, distd.;

Reference yield:

→ Dimethylgermanium-difluorid (811-70-1)

Guidance literature:

Me2GeBr2, SbF3;

DOI:10.1016/S0022-328X(00)84039-5

Refernces