C₁₇H₁₂ClN

Base Information

• Chemical Name: C₁₇H₁₂ClN
• CAS No.: 1174895-49-8
• Molecular Formula: C₁₇H₁₂ClN
• Molecular Weight: 265.742
• Mol file: 1174895-49-8.mol

Synonyms:C₁₇H₁₂ClN

Chemical Property of C₁₇H₁₂ClN

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₁₇H₁₂ClN

There total 2 articles about C₁₇H₁₂ClN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2-phenylpyridine (1008-89-5) + m-chlorobenzoyl peroxide (845-30-7) → C17H12ClN (1174895-49-8)

Guidance literature:

With palladium diacetate; In acetic acid; acetonitrile; for 2h; Heating; Inert atmosphere;

DOI:10.1021/ol900756g

Reference yield: 45.0%

2-phenylpyridine (1008-89-5) + m-Chlorobenzaldehyde (587-04-2) → C17H12ClN (1174895-49-8) + C23H15Cl2N (1245266-40-3)

Guidance literature:

With acetylacetonatodicarbonylrhodium(l); di-tert-butyl peroxide; In chlorobenzene; at 150 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ja105396b

upstream raw materials:

2-phenylpyridine

m-chlorobenzoyl peroxide

m-Chlorobenzaldehyde

Refernces

• 1、 Yu, Wing-Yiu,Sit, Wing Nga,Zhou, Zhongyuan,Chan, Albert S.-C.. "Palladium-catalyzed decarboxylative arylation of C-H bonds by aryl acylperoxides". supporting information; experimental part. p. 3174 - 3177. Retrieved 2009/11/30.