MCL-693

Base Information

• Chemical Name: MCL-693
• CAS No.: 1310086-87-3
• Molecular Formula: C₃₉H₅₃NO₅
• Molecular Weight: 615.854
• Mol file: 1310086-87-3.mol

Synonyms:MCL-693

Chemical Property of MCL-693

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of MCL-693

There total 6 articles about MCL-693 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

MCL-691 (1310086-72-6) + decanedioic acid monobenzyl ester (67852-88-4) → MCL-693 (1310086-87-3)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane;

DOI:10.1016/j.bmc.2011.03.052

Reference yield:

MCL-691 (1310086-72-6) + monobenzyl sebacoyl chloride (67852-87-3) → MCL-693 (1310086-87-3)

Guidance literature:

With triethylamine; In dichloromethane;

DOI:10.1016/j.bmc.2011.03.052

Reference yield:

MCL 499 (1064078-15-4) → MCL-693 (1310086-87-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 20 °C

1.2: 1 h / 20 °C

2.1: palladium on carbon; hydrogen / methanol / 20 °C

3.1: dmap; dicyclohexyl-carbodiimide / dichloromethane

With dmap; palladium on carbon; hydrogen; sodium hydride; dicyclohexyl-carbodiimide; In methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;

DOI:10.1016/j.bmc.2011.03.052

upstream raw materials:

MCL 499

C₂₉H₃₇NO₂

MCL-691

decanedioic acid monobenzyl ester

Refernces