N,N‘-di(4-chlorophenyl)phthaldiamide

Base Information

• Chemical Name: N,N‘-di(4-chlorophenyl)phthaldiamide
• CAS No.: 20171-91-9
• Molecular Formula: C₂₀H₁₄Cl₂N₂O₂
• Molecular Weight: 385.249
• Mol file: 20171-91-9.mol

Synonyms:N,N‘-di(4-chlorophenyl)phthaldiamide

Chemical Property of N,N‘-di(4-chlorophenyl)phthaldiamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N‘-di(4-chlorophenyl)phthaldiamide

There total 2 articles about N,N‘-di(4-chlorophenyl)phthaldiamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

4-chloro-aniline (106-47-8) + Phthaloyl dichloride (88-95-9) → N,N‘-di(4-chlorophenyl)phthaldiamide (20171-91-9)

Guidance literature:

In diethyl ether; at 20 ℃; for 16h;

DOI:10.1002/chem.201705578

Reference yield:

→ N,N‘-di(4-chlorophenyl)phthaldiamide (20171-91-9)

Guidance literature:

DOI:10.1021/je60039a033

Reference yield: 65.0%

N,N‘-di(4-chlorophenyl)phthaldiamide (20171-91-9) → 2,3-di(4-chlorophenyl)-2,3-dihydrophthalazin-1,4-dione

Guidance literature:

With tert-butylammonium hexafluorophosphate(V); Electrolysis;

DOI:10.1002/chem.201705578

upstream raw materials:

4-chloro-aniline

Phthaloyl dichloride

Downstream raw materials:

N-(4-chlorophenyl)phthalimide

bis-(4-chloro-phenyl)-diazene

Refernces