1,2,3,4-tetrahydro-9-anthranol

Base Information

• Chemical Name: 1,2,3,4-tetrahydro-9-anthranol
• CAS No.: 50703-94-1
• Molecular Formula: C₁₄H₁₄O
• Molecular Weight: 198.265
• Mol file: 50703-94-1.mol

Synonyms:1,2,3,4-tetrahydro-9-anthranol

Chemical Property of 1,2,3,4-tetrahydro-9-anthranol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,2,3,4-tetrahydro-9-anthranol

There total 2 articles about 1,2,3,4-tetrahydro-9-anthranol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9,10-phenanthrenequinone (84-65-1) → anthracene (120-12-7) + anthracen-9(10H)-one (90-44-8) + 1,2,3,4-tetrahydro-9,10-anthraquinone (4923-66-4) + 1,2,3,4-tetrahydro-9-anthranol (50703-94-1)

Guidance literature:

With sodium tetrahydroborate; hydrogen; nickel dichloride; In isopropyl alcohol; at 60 - 70 ℃; for 10h;

DOI:10.1134/S1070363214090023

Reference yield:

9,10-phenanthrenequinone (84-65-1) + decalin (91-17-8) → anthracene (120-12-7) + tetradecahydroanthracene (6596-35-6) + 1,2,3,4-tetrahydro-9-anthranol (50703-94-1) + 9-Hydroxy-1.2.3.4.5.6.7.8-octahydro-anthracen (110836-01-6)

Guidance literature:

at 160 - 170 ℃; unter hohem Druck, 8 Atome Wasserstoff_.Hydrogenation;

Reference yield:

1,2,3,4-tetrahydro-9-anthranol (50703-94-1) + decalin (91-17-8) → 1,2,3,4,5,6,7,8-octahydroanthracene (1079-71-6)

Guidance literature:

at 160 - 170 ℃; Hydrogenation;

upstream raw materials:

9,10-phenanthrenequinone

decalin

Downstream raw materials:

ethanol

1,2,3,4,5,6,7,8-octahydroanthracene

Refernces